Faculty Profiles - MIKAMI Takashi

写真a

MIKAMI Takashi

Organization

Academic Assembly Institute of Science and Technology SEISAN DESIGN KOUGAKU KEIRETU Associate Professor
Graduate School of Science and Technology Advanced Materials Science and Technology Associate Professor
Faculty of Engineering Department of Engineering Associate Professor

Homepage

http://crystallization.eng.niigata-u.ac.jp/

External link

Degree

学士（工学） ( 2005.3 早稲田大学 )
修士（工学） ( 2007.3 早稲田大学 )
博士（工学） ( 2010.3 早稲田大学 )

Research Interests

化学工学
晶析工学

Research Areas

Manufacturing Technology (Mechanical Engineering, Electrical and Electronic Engineering, Chemical Engineering) / Transport phenomena and unit operations

Research History (researchmap)

Niigata University Faculty of Engineering Department of Engineering Associate Professor

2017.4

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Niigata University Graduate School of Science and Technology Advanced Materials Science and Technology Associate Professor

2013.4

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Niigata University Faculty of Engineering Department of Chemistry and Chemical Engineering Chemical Engineering Associate Professor

2013.4 - 2017.3

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Tsuruoka National College of Technology Assistant Professor

2010.4 - 2013.3

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日本学術振興会特別研究員 DC2（工学）

2009.4 - 2010.3

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Waseda University Faculty of Science and Engineering Research Assistant

2008.10 - 2009.3

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Research History

Niigata University Faculty of Engineering Department of Engineering Associate Professor

2017.4
Niigata University Graduate School of Science and Technology Advanced Materials Science and Technology Associate Professor

2013.4
Niigata University Abolition organization Chemical Engineering Associate Professor

2013.4 - 2017.3

Education

Waseda University 先進理工学研究科応用化学専攻

- 2010.3

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Country： Japan

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Waseda University Graduate School, Division of Science and Engineering 応用化学専攻

- 2007.3

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Country： Japan

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Waseda University Faculty of Science and Engineering 応用化学科

- 2005.3

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Country： Japan

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Professional Memberships

化学工学会

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分離技術会

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日本工学教育協会

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Papers

Influence of Feed Condition on Crystal Size Distribution of Potassium Alum Obtained by Unseeded Two-Stage Semi-Batch Cooling Crystallization Reviewed

Takashi Mikami, Rika Kaizu

JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 52 ( 3 ) 317 - 324 2019.3

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Authorship：Lead author,　Corresponding author Publishing type：Research paper (scientific journal) Publisher：Society of Chemical Engineers, Japan

DOI： 10.1252/jcej.18we122

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Influence of Feed Condition on Crystal Size Distribution of Potassium Alum Obtained by Unseeded Semi-batch Cooling Crystallization Reviewed

Takashi Mikami, Rika Kaizu, Tetsu Saito

JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 51 ( 5 ) 454 - 459 2018.5

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Authorship：Lead author,　Corresponding author Publishing type：Research paper (scientific journal) Publisher：Society of Chemical Engineers, Japan

DOI： 10.1252/jcej.17we142

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Reactive Crystallization of Lithium Carbonate in the Presence of Magnesium Impurity Reviewed

Takashi Mikami, Tadashi Koseki

Journal of Chemical Engineering of Japan 50 ( 4 ) 309 - 314 2017

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Authorship：Lead author,　Corresponding author Language：English Publishing type：Research paper (scientific journal) Publisher：Society of Chemical Engineers, Japan

DOI： 10.1252/jcej.16we150

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Heterogeneous Precipitation of Gold Nanoparticles on PEI Coated Silica Gel Reviewed

Takashi Mikami, Chisato Konno, Yuta Takayasu, Izumi Hirasawa

Journal of Chemical Engineering of Japan 49 ( 2 ) 186 - 190 2016

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Authorship：Lead author Language：English Publishing type：Research paper (scientific journal) Publisher：Society of Chemical Engineers, Japan

Gold nanoparticles were precipitated on the surface of silica gel without mechanical mixing. Polyethylenimine (PEI) which was coated on the surface of silica gel reduced raw materials of hydrogen tetrachloroaurate (III) tetrahydrate (HAuCl44H2O). Formation of gold nanoparticles on silica gel was confirmed by using Field Emission Scanning Electron Microscope (FE-SEM) and Energy Dispersive X-ray Fluorescence Spectrometer (EDX). In this study, particles size distribution and coverage ratio of gold on silica gel were investigated.

DOI： 10.1252/jcej.15we065

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Kinetic Study on Polyethylenimine-Assisted Reactive Crystallization of Monodisperse Strontium Sulfate Microcrystals Reviewed

Takashi Mikami, Izumi Hirasawa

Chemical Engineering & Technology 36 ( 8 ) 1320 - 1326 2013.8

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Authorship：Lead author Language：English Publishing type：Research paper (scientific journal) Publisher：Wiley

Double-jet reactive crystallization of SrSO4 was carried out in the presence of polyethylenimine (PEI). A simple kinetic model of primary nucleation as well as crystal growth was investigated under the condition of producing monodisperse microcrystals. Furthermore, surface free energy in the solution of PEI was estimated. PEI addition causes growth inhibition leading to smaller sizes and modifies the Gibbs free energy gap required for occurring nucleation.

DOI： 10.1002/ceat.201200276

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Single-Jet Precipitation of Silver Nanocrystals in the Presence of Poly(acrylic) Acid Reviewed

Takashi Mikami, Takahiro Nagahori, Jin Saito, Izumi Hirasawa

Chemical Engineering & Technology 35 ( 4 ) 700 - 704 2012.4

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Authorship：Lead author Publishing type：Research paper (scientific journal) Publisher：Wiley

DOI： 10.1002/ceat.201100460

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Influence of Polyethyleneimine Addition on Crystal Size Distribution of Au Nanocrystals Reviewed

Takashi Mikami, Yuta Takayasu, Junpei Watanabe, Izumi Hirasawa

Chemical Engineering & Technology 34 ( 4 ) 583 - 586 2011.4

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Authorship：Lead author Publishing type：Research paper (scientific journal) Publisher：Wiley

DOI： 10.1002/ceat.201000495

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CSD-controlled reactive crystallization of SrSO4 in the presence of polyethylenimine Reviewed

Takashi Mikami, Takahiro Sakuma, Izumi Hirasawa

Chemical Engineering Research and Design 88 ( 9 ) 1200 - 1205 2010.9

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Authorship：Lead author Publishing type：Research paper (scientific journal) Publisher：Elsevier BV

DOI： 10.1016/j.cherd.2010.01.030

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PEI-assisted preparation of Au nanoparticles via reductive crystallization process Reviewed

Takashi Mikami, Yuta Takayasu, Izumi Hirasawa

Chemical Engineering Research and Design 88 ( 9 ) 1248 - 1251 2010.9

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Authorship：Lead author Publishing type：Research paper (scientific journal) Publisher：Elsevier BV

DOI： 10.1016/j.cherd.2009.08.013

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Polyelectrolyte-Assisted Reactive Crystallization of SrSO4 to Obtain Monodispersed Nano/Micro-Particles Reviewed

Takashi Mikami, Izumi Hirasawa

Chemical Engineering & Technology 33 ( 5 ) 797 - 803 2010.4

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Authorship：Lead author Language：English Publishing type：Research paper (scientific journal) Publisher：Wiley

Micronized SrSO4 crystals having monodispersed/narrow distributions were produced with a controlled double-jet reactive crystallizer. Polyethylenimine (PEI) had the role of a suitable controller of supersaturation and following crystallization phenomena, and then led to agglomeration-less homogeneous crystalline qualities. Especially, the PEI imines seemed to adjust the number of nucleates, and also physical gel networks seemed to contribute to the inhibition of further particulate agglomeration. The current paper mainly demonstrated the influence of PEI addition on the resulting properties, e.g. sizes and size distribution widths. Therefore the polyelectrolyte-assisted technique will develop as a build-up process contributing to provide high-value nano/micro-powders having the desired crystalline qualities.

DOI： 10.1002/ceat.200900544

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Quality-Controlled Reactive Crystallization of SrSO4 To Produce High-Valued Chemicals Reviewed

Takashi Mikami, Izumi Hirasawa

Chemical Engineering & Technology 33 ( 5 ) 775 - 779 2010.4

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Authorship：Lead author Language：English Publishing type：Research paper (scientific journal) Publisher：Wiley

Precipitation of monodispersed SrSO4 particles was carried out in the presence of polyethylenimine (PEI). PEI additions varied some particulate properties, e.g., sizes, shapes, size distribution widths, and agglomeration ratios. The present paper mainly focuses on the influence of PEI dosage on crystal size distributions. PEI-assisted double jet techniques require no difficult controls of feeding rates, therefore, this idea will be applicable to precipitation of other inorganic compounds for the purpose of producing monodispersed nano-/microparticles.

DOI： 10.1002/ceat.200900545

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Influence of Polyethylenimine on Double-Jet Reactive Crystallization Process of Monodisperse BaSO4 Reviewed

Takashi Mikami, Shota Ikeda, Izumi Hirasawa

JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 43 ( 8 ) 698 - 703 2010

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Authorship：Lead author Language：English Publishing type：Research paper (scientific journal) Publisher：Society of Chemical Engineers, Japan

Micronized BaSO4 particles with a narrow size distribution were produced by using a double-jet reactive crystallizer. Polyethylenimine (PEI) acted as a growth/agglomeration inhibitor at a high PEI dosage, hence the particle size and size distribution width decreased, and BaSO4 crystals with the desired qualities were obtained. Similar results were obtained in previous studies in which of SrSO4 and PbSO4. We believe that our method, which involves the use of PEI, can be employed for the production of various inorganic sulfates in which the particles have a monodisperse size distribution.

DOI： 10.1252/jcej.09we218

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Control of CSD Width via PEI-Assisted Reactive Crystallization of Micro-SrSO4 Particles Reviewed

Takashi Mikami, Izumi Hirasawa

JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 43 ( 3 ) 308 - 312 2010

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A controlled double-jet reactive crystallization technique using a PEI (polyethylenimine) additive has been conducted to produce agglomeration-free micro-particles of SrSO4 with narrow and mono-dispersed size distributions. PEI successfully inhibits rapid/continuous nucleation due to a complexation with strontium ions before nucleation occurs, and enables realization of perfect separation of nucleation and growth. Our idea to obtain fine particles with desired size distributions will introduce a new potential for contributing to enhance high-valued material properties.

DOI： 10.1252/jcej.09we112

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Effect of Feeding Condition on Crystal Size Distributions of Mono-Dispersed SrSO4 Particles Produced via PEI-Assisted Double-Jet Reactive Crystallization Reviewed

Takashi Mikami, Takahiro Sakuma, Izumi Hirasawa

JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 43 ( 3 ) 300 - 307 2010

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Micron-sized SrSO4 particles having mono-dispersed/narrow distributions have been produced with a double-jet semi-batch reactive crystallizer. Slow molar feedings over a short time maintained proper supersaturation levels and result in narrow distributions due to the prevention of agglomeration growth of small primary precipitates. Furthermore, polyethylenimine (PEI) is a suitable growth/agglomeration inhibitor for sulfate precipitation, e.g., SrSO4 and PbSO4, and effectively reduced particle sizes leading to single-micron products. Besides feeding conditions, in the present work, the influence of PEI dosage on crystal size distributions (CSDs) is investigated. The controlled double-jet feeding using a polyelectrolyte additive such as PEI will be a powerful methodology to obtain agglomeration-free uniform micro-powders as a final solid product.

DOI： 10.1252/jcej.09we113

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反応晶析プロセスを利用した単分散硫酸塩の製造

三上貴司, 平沢泉

化学工学会研究発表講演要旨集 2009 434 - 434 2009

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Language：Japanese Publisher：公益社団法人化学工学会

DOI： 10.11491/scej.2009f.0.434.0

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難溶解性塩の反応晶析系における添加剤の影響

三上貴司, 平沢泉

化学工学会研究発表講演要旨集 2008 697 - 697 2008

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Language：Japanese Publisher：公益社団法人化学工学会

DOI： 10.11491/scej.2008.0.697.0

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熟成過程における硫酸ストロンチウム微粒子特性の挙動について

三上貴司, 池田将太, 平沢泉

化学工学会研究発表講演要旨集 2007 96 - 96 2007

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Language：Japanese Publisher：公益社団法人化学工学会

DOI： 10.11491/scej.2007.0.96.0

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高分子電解質反応場における硫酸バリウム単分散微粒子生成手法に関する考察

池田将太, 中江翼, 三上貴司, 平沢泉

化学工学会研究発表講演要旨集 2007 97 - 97 2007

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Language：Japanese Publisher：公益社団法人化学工学会

DOI： 10.11491/scej.2007.0.97.0

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Strategy to Obtain nm Size Crystals through Precipitation in the Presence of Polyelectrolyte Reviewed

Izumi Hirasawa, Takashi Mikami, Akio Katayama, Takahiro Sakuma

Chemical Engineering & Technology 29 ( 2 ) 212 - 214 2006.2

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Publishing type：Research paper (scientific journal) Publisher：Wiley

DOI： 10.1002/ceat.200500355

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高分子電解質反応場を利用した硫酸ストロンチウムの単分散微粒子生成

三上貴司, 丸山裕一, 池田将太, 平沢泉

化学工学会研究発表講演要旨集 2006 83 - 83 2006

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Language：Japanese Publisher：公益社団法人化学工学会

DOI： 10.11491/scej.2006f.0.83.0

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高分子凝集抑制剤を用いた反応晶析法による硫酸ストロンチウム結晶の単分散微粒子生成プロセスに関する研究

佐久間崇浩, 三上貴司, 平沢泉

化学工学会研究発表講演要旨集 2005 98 - 98 2005

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Language：Japanese Publisher：公益社団法人化学工学会

DOI： 10.11491/scej.2005.0.98.0

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Books

分離プロセスの最適化とスケールアップの進め方

技術情報協会（ Role： Joint author）

技術情報協会 2019.11 （ ISBN:9784861047664 ）

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Total pages：634p Language：Japanese

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晶析工学は、どこまで進歩したか

化学工学会, 化学工学会材料界面部会晶析技術分科会（ Role： Joint author）

化学工学会関東支部,三恵社 (発売) 2015.1 （ ISBN:9784864873253 ）

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Total pages：vi, 208p Language：Japanese

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分離技術のシーズとライセンス技術の実用化

三上貴司（ Role： Joint author , 単分散微結晶の反応晶析技術（pp.15-22））

分離技術会 2014.10

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Language：Japanese Book type：Scholarly book

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MISC

医薬品原薬の回分冷却晶析工程における溶媒組成および過飽和度の影響

石川大樹, 伊藤康広, 三上貴司

鶴岡工業高等専門学校紀要 47 59 - 64 2013.3

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (bulletin of university, research institution) Publisher：鶴岡工業高等専門学校

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単分散微結晶の反応晶析技術

三上貴司

鶴岡工業高等専門学校紀要 46 83 - 88 2012.2

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (bulletin of university, research institution) Publisher：鶴岡工業高等専門学校

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晶析操作による結晶品質制御

三上貴司

鶴岡工業高等専門学校紀要 45 65 - 73 2011.3

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (bulletin of university, research institution) Publisher：鶴岡工業高等専門学校

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高分子電解質環境場を利用した単分散微結晶の反応晶析

三上貴司

分離技術会誌 41 ( 2 ) 105 - 111 2011.2

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (other) Publisher：分離技術会

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反応晶析プロセスを利用した単分散硫酸塩の製造（その2）

三上貴司, 平沢泉

硫酸と工業 63 ( 6 ) 1 - 5 2010.6

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (other) Publisher：硫酸協会

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Reactive crystallization of mono-dispersed sulfates (part 2)

Sulphuric acid and industry. 63 ( 6 ) 83 - 87 2010.6

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Language：Japanese

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反応晶析プロセスを利用した単分散硫酸塩の製造（その1）

三上貴司, 平沢泉

硫酸と工業 63 ( 5 ) 1 - 7 2010.5

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (other) Publisher：硫酸協会

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Reactive crystallization of mono-dispersed sulfates (part 1)

Sulphuric acid and industry. 63 ( 5 ) 69 - 75 2010.5

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Crystallization Technology to Create Nanocrystals

HIRASAWA Izumi, MIKAMI Takashi

Journal of the Japan Society of Colour Material 81 ( 5 ) 161 - 164 2008.5

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (other) Publisher：Japan Society of Colour Material

DOI： 10.4011/shikizai.81.161

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晶析工学を基軸にしたナノ結晶のビルドアップ

平沢泉, 三上貴司, 池田将太

ケミカルエンジニヤリング 52 ( 3 ) 222 - 226 2007.3

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Language：Japanese Publishing type：Article, review, commentary, editorial, etc. (trade magazine, newspaper, online media) Publisher：化学工業社

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Awards

インテリジェント・コスモス奨励賞

2012.5 インテリジェント・コスモス学術振興財団

三上貴司

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Award type：Award from publisher, newspaper, foundation, etc. Country：Japan

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早稲田大学水野賞

2010.3 早稲田大学

三上貴司

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Country：Japan

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化学工学会室蘭大会ポスター賞

2006.8 化学工学会

三上貴司

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Award type：Award from Japanese society, conference, symposium, etc. Country：Japan

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Research Projects

晶析工学を基軸にした有機物造粒晶の製造

2020.4 - 2021.3

System name：令和2年度研究助成

Awarding organization：公益財団法人新潟工学振興会

三上貴司

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冷却晶析操作の新規概念に基づく単分散結晶の製造

2016.4 - 2020.3

System name：科学研究費助成事業

Research category：若手研究(B)

Awarding organization：日本学術振興会

三上貴司

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Authorship：Principal investigator Grant type：Competitive

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Effects of composition and flow of solution on the production of calcium phosphates on titanium

Grant number：15K06436

2015.4 - 2018.3

System name：Grants-in-Aid for Scientific Research

Research category：Grant-in-Aid for Scientific Research (C)

Awarding organization：Japan Society for the Promotion of Science

KIMURA Isao

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Grant amount：\4940000 （ Direct Cost: \3800000 、 Indirect Cost：\1140000 ）

The optimum composition of the reactant solution in a process for producing calcium phosphates (CaP) on a titanium plate was studied based on a simulated body fluid (SBF). In particular, the effect of magnesium ion concentration was investigated, and consequently a condition under which CaP can be produced within a duration shorter than using SBF was found. Coexisting species for controlling the morphology was investigated. The effect of ordered alterations in height of the effective space of a small reactor on the flow of SBF was discussed. Microcapsules to compensate the decrease in calcium ions which have been deposited as CaP were prepared by dispersion polymerization, and their releasing property was characterized.

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マグネシウム存在下における高品位炭酸リチウムの反応晶析研究

2014.4 - 2015.3

System name：平成26年度研究助成

Awarding organization：公益財団法人ソルト・サイエンス研究財団

三上貴司

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Authorship：Principal investigator Grant type：Competitive

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医薬品有効成分の回分冷却晶析研究

2014.4 - 2015.3

System name：試験研究費助成

Awarding organization：公益財団法人内田エネルギー科学振興財団

三上貴司

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Authorship：Principal investigator Grant type：Competitive

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海水中リチウム資源の高品位化回収に関する反応晶析研究

2012.4 - 2013.3

System name：平成24年度研究助成

Awarding organization：公益財団法人ソルト・サイエンス研究財団

三上貴司

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晶析工学を基軸とした資源循環型無機排水処理プロセスの開発

2012.4 - 2013.3

System name：平成24年度研究助成

Awarding organization：公益財団法人畠山文化財団

三上貴司

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Grant type：Competitive

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晶析工学を基軸とした資源循環型重金属イオン回収プロセスの開発

2010.4 - 2012.3

System name：平成22年度環境助成研究

Awarding organization：財団法人鉄鋼業環境保全技術開発基金

三上貴司

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晶析工学を基軸にした単分散微粒子製法の開発

2010.4 - 2012.3

System name：科学研究費助成事業

Research category：若手研究(スタートアップ)

三上貴司

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Authorship：Principal investigator Grant type：Competitive

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単分散微粒子の製法に関する工業晶析研究

2009.4 - 2010.3

System name：科学研究費助成事業

Research category：特別研究員推奨費

三上貴司

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Authorship：Principal investigator Grant type：Competitive

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Teaching Experience (researchmap)

反応装置工学

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卒業研修

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論文輪講I

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卒業研究

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工学リテラシー入門（化学材料分野）

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化学工学

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工業英語

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物質化学実験（化学工学）

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物質化学実験（分析化学）

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創造実習

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応用化学基礎演習（反応工学）

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理工学基礎実験（物理化学）

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工業分析化学

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物質工学概論

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素材生産科学文献詳読Ⅱ

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粉体工学特論

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分離工学演習

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化学工学実験

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粉粒体工学

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精密粉粒体工学

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工学リテラシー入門（化学システム工学科）

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素材生産科学セミナーⅡ

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材料プロセス工学

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素材生産科学セミナーⅠ

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材料生産システム特定研究Ⅰ

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化学実験

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素材生産科学特別演習

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設計製図

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研究発表演習・発表

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素材生産科学文献詳読Ⅰ

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技術英語入門

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材料生産システム特定研究Ⅱ

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粉体工学

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Teaching Experience

設計製図

2022
Institution name：新潟大学
機械的分離工学

2022
Institution name：新潟大学
拡散操作III

2022
Institution name：新潟大学
リメディアル演習

2022
Institution name：新潟大学
技術文献リサーチC

2020
Institution name：新潟大学
技術文献リサーチB

2020
Institution name：新潟大学
技術文献リサーチA

2020
Institution name：新潟大学
技術文献リサーチD

2020
Institution name：新潟大学
化学実験2

2019
Institution name：新潟大学
リメディアル演習

2019

-

2022
Institution name：新潟大学
化学実験1

2018
Institution name：新潟大学
卒業研究

2018
Institution name：新潟大学
卒業研修

2017
Institution name：新潟大学
工学リテラシー入門(化学材料分野)

2017
Institution name：新潟大学
論文輪講I

2017

-

2019
Institution name：新潟大学
論文輪講II

2017

-

2018
Institution name：新潟大学
反応装置工学

2016
Institution name：新潟大学
粉体工学

2016
Institution name：新潟大学
技術英語入門

2016
Institution name：新潟大学
素材生産科学文献詳読Ⅱ

2015
Institution name：新潟大学
材料生産システム特定研究Ⅱ

2015
Institution name：新潟大学
素材生産科学セミナーⅡ

2015
Institution name：新潟大学
材料プロセス工学

2014

-

2020
Institution name：新潟大学
設計製図

2014

-

2016
Institution name：新潟大学
研究発表演習・発表

2014

-

2015
Institution name：新潟大学
素材生産科学文献詳読Ⅰ

2014

-

2015
Institution name：新潟大学
素材生産科学特別演習

2014

-

2015
Institution name：新潟大学
材料生産システム特定研究Ⅰ

2014

-

2015
Institution name：新潟大学
素材生産科学セミナーⅠ

2014

-

2015
Institution name：新潟大学
化学工学実験

2013
Institution name：新潟大学
粉体工学特論

2013
Institution name：新潟大学
精密粉粒体工学

2013
Institution name：新潟大学
分離工学演習

2013

-

2021
Institution name：新潟大学
化学実験

2013

-

2020
Institution name：新潟大学
工学リテラシー入門(化学システム工学科)

2013

-

2020
Institution name：新潟大学
粉粒体工学

2013

-

2020
Institution name：新潟大学

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